采用吹扫捕集-顶空气相色谱法(P&T-GC)和顶空气相色谱法(HS-GC)对卷烟包装材料中残留的挥发性有机物进行检测,结果表明,P&T-GC方法的检出限为0.015～0.42ng/cm2,平均回收率91.3%～99.4%,相对标准偏差0.17%～2.74%;HS-GC方法的检出限为0.20～7.00ng/cm2,平均回收率89.1%～99.2%,相对标准偏差0.96%～3.23%;P&T-GC法比HS-GC法增加了对异丙苯、苯乙烯和苯甲醛的检测,并且P&T-GC方法能使间二甲苯和对二甲苯分离并准确定量;利用P&T-GC法检测到卷烟包装材料中残留的挥发性有机物含量要比HS-GC法高;P&T-GC法更适合用于包装材料质量控制。 The residual volatile organic compounds in cigarette packaging materials were detected by P & T-GC and headspace gas chromatography (HS-GC). The results showed that the detection of P & T-GC The average recovery was from 91.3% to 99.4% and the relative standard deviation was from 0.17% to 2.74%. The detection limits were 0.20-7.00ng / cm2 for HS-GC and the average recoveries were from 89.1% to 99.2% %, And the relative standard deviations (RSDs) ranged from 0.96% to 3.23%. The detection of cumene, styrene and benzaldehyde was increased by P & T-GC method compared with HS-GC method. And accurate quantification; using P & T-GC method to detect residual volatile organic compounds in cigarette packaging material than HS-GC method; P & T-GC method is more suitable for packaging material quality control.