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采用界面聚合法合成了聚(1-萘胺)纳米颗粒。利用红外光谱(FT-IR),紫外可见吸收光谱(UV-vis),电子扫描显微镜(SEM),投射电镜(TEM),X射线衍射(XRD),循环伏安(cyclic voltammogram)等测试方法,对聚合物进行了表征并对聚合物形貌、结构及性能进行了初步探讨。结果表明,界面聚合法合成的聚(1-萘胺)呈现直径在100nm内的颗粒状分布;XRD结果显示,聚(1-萘胺)为半结晶态聚合物;界面聚合法合成的聚(1-萘胺)具有一定的电化学活性。
Poly (1-naphthylamine) nanoparticles were synthesized by interfacial polymerization. The microstructure and mechanical properties were characterized by FT-IR, UV-vis, SEM, TEM, XRD and cyclic voltammogram. The polymer was characterized and the polymer morphology, structure and properties were discussed. The results showed that the poly (1-naphthylamine) synthesized by the interfacial polymerization showed a granular distribution with a diameter of 100 nm. The XRD results showed that the poly (1-naphthylamine) 1-naphthylamine) has a certain electrochemical activity.