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A new iodiplumbate polymer [(AOD)(Pb2I6)]n 1 (AOD = O-protonated 4-azonia-7-oxaspiro(4,5) decane quaternary ammonium) was synthesized by self-assembly reaction of AOD·I, Pb(NO3)2 and NaI, and structurally determined. Compound 1 crystallizes in the he