We used a rectangular waveguide system to measure the X-band (8-12 GHz) transmission of hexagon split ring resonators (SRRs) alone and the left-handed metamaterials (LHMs) consisting of hexagon SRR array and wire array. The experimental results show that for an individual SRR, the resonance frequency increases with the azimuthal gap, but decreases with the radial gap. For two identical SRRs, the resonance peak has a shift because of the electromagnetic interaction, and the resonance frequency and the strength decrease with the separation distance. Finally, we demonstrate the left-handed effect of the LHMs.