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为了获得抗流失性木材阻然剂.并为实现木材工业化的阻燃处理.首先以廉价的尿素为原料、合成了一经甲基脲(HMU);对HMU、蜜胺(MA)、磷酸氢二铵(DAP)的配比、处理木材的压力、时间进行了正交实验;测定了阻燃木材的载药率和氧指数以及阻燃剂的抗浸提值。结果表明:影响阻燃性的显著因子是浸药时间.三组分配比影响最小,HMU、MA、DAP的较佳配比为5:1:6.5。较佳的阻燃处理条件:压力为600~1300Pa,时间为30h左右、温度为50℃。当兴安落叶松载药率为0.63%时,氧指数达到30,抗浸提值为36.88%。该木材阻燃剂具有较好的阻燃性和一定的抗流失性,所选择的阻燃处理条件可作为工业生产的参考。
In order to obtain resistance to loss of wood resistance agent. And for the realization of wood industrial flame retardant treatment. First of all, urea (urea) was used as a raw material to synthesize a methyl urea (HMU). The orthogonal experiment was carried out on the ratio of HMU, melamine (MA) and diammonium phosphate (DAP) The loading rate and oxygen index of flame-retardant wood and the anti-leaching value of flame retardant were determined. The results show that: a significant factor affecting the flame retardancy is the soaking time. The three groups had the least impact on the ratio of HMU, MA and DAP, which was 5: 1: 6.5. The preferred flame retardant treatment conditions: a pressure of 600 ~ 1300Pa, a time of about 30h, a temperature of 50 ℃. When the loading rate of Larix gmelinii was 0.63%, the oxygen index reached 30, anti-leaching value of 36.88%. The wood flame retardant has a good flame retardancy and a certain resistance to loss, the selected flame retardant processing conditions can be used as a reference for industrial production.