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报道了三价磷化合物与亲电氟化试剂Selectfluor的氟化反应,反应以乙腈/水为溶剂、室温条件下反应15~60min,以34%~81%的收率得到了磷酰氟类化合物.
The fluorination reaction of trivalent phosphorus compounds with Selectfluor was reported. The reaction was carried out with acetonitrile / water as solvent at room temperature for 15 ~ 60 min, and the yield of phosphoryl fluoride was 34% ~ 81% .