分散紫107(C.I.Disperse Violet 107)的合成

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以4-氨基-N-甲基邻苯二甲酰亚胺为原料,经溴化、过滤,制得溴化物4-氨基-5-溴-N-甲基邻苯二甲酰亚胺;然后以该溴化物为原料用亚硝酸钠进行重氮化,制得的重氮溶液与3-N,N-二乙氨基乙酰苯胺偶合,生成偶合物,再进行水洗、过滤,所得的滤饼经干燥、粉碎,进行氰基取代反应,该反应使用DMF做溶剂,用氰化钠在无水条件下进行,合成出的滤饼经3次DMF洗涤、3次工艺水洗涤,去除副产物而制得高牢度的分散染料.研究了反应条件的影响,在优化条件下,总收率93.64%.
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