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以NiCl2·6H2O和C4H9NH2·HCl为原料,利用固相合成法成功合成了层状结构的有机/无机杂化物(C4H9NH3)2NiCl4(1);采用X射线粉末衍射仪和红外光谱仪表征了产物1的结构,利用元素分析和热重分析测定了其元素组成和热稳定性.结果表明,杂化物1具有层状结构,层间距为3.220 7nm.
The layered organic / inorganic hybrid (C4H9NH3) 2NiCl4 (1) was successfully synthesized by solid-phase synthesis using NiCl2 · 6H2O and C4H9NH2 · HCl as raw materials. The product 1 was characterized by X-ray powder diffraction and infrared spectroscopy Structure and the elemental composition and thermal stability were measured by elemental analysis and thermogravimetric analysis.The results show that the hybrid 1 has a layered structure with a layer spacing of 3.220 7 nm.