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样品经甲醇提取,在硅胶G薄层板上,以石油醚(60~90℃)—乙酸乙酯(9.5∶0.5)展开,激发波长λEX=313nm,线性范围1~8μg,平均回收率101.3%,RSD=3.2%。
The sample was extracted with methanol, and developed on silica gel G-thin layer plate. It was developed with petroleum ether (60-90°C)-ethyl acetate (9.5:0.5). The excitation wavelength λEX=313 nm, and the linear range was 1-8 μg. The recovery rate was 101.3% and RSD = 3.2%.