Enhanced magnetic properties in Nd-Fe-B magnets prepared by spark plasma sintering via die-upsetting

来源 :Journal of Rare Earths | 被引量 : 0次 | 上传用户:syyyqw
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The magnetic properties and microstructure of Nd-Fe-B magnets prepared by spark plasma sintering with different die-upsetting processes were investigated. The results showed that the optimum magnetic properties of die-upset Nd-Fe-B magnets were obtained at 680 ℃ when the die-upset level was 60%, and the degree of magnetic alignment was 0.84. The microstructures showed that the coarse grains oc-curred predominantly within certain areas, and abnormal grain growth was not observed within the major areas of well-aligned grains. There existed many small spherical grains, which stacked together and were not aligned during die upsetting when the deformation temperature was 650 ℃. These small spherical grains grew up, and were aligned when the deformation temperature increased from 650 to 680 ℃, which could improve the crystallographic alignment of die-upset Nd-Fe-B magnets. The magnetic properties and microstructure of Nd-Fe-B magnets prepared by spark plasma sintering with different die-upsetting processes were investigated. When results that the optimum magnetic properties of die-upset Nd-Fe-B magnets were obtained at 680 ℃ when the die-upset level was 60%, and the degree of magnetic alignment was 0.84. The microstructures showed that the coarse grains oc-curred predominantly within certain areas, and abnormal grain growth was not observed within the major areas of well-aligned grains. Which had many small spherical grains, which stacked together and were not aligned during die upsetting when the deformation temperature was 650 ° C. These small spherical grains grew up, and were aligned when the deformation temperature increased from 650 to 680 ° C, which could improve the crystallographic alignment of die-upset Nd-Fe-B magnets.
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