PREPARATION OF NANOMETER ZINC OXIDE BY EVAPORATION METHOD

来源 :Acta Metallurgica Sinica(English Letters) | 被引量 : 0次 | 上传用户:xiaozhao550
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Nanometer ZnO particles were synthesized by evaporating of zinc powders of averageparticle size of 370μm studied by XRD, TEM and electron diffraction. The particleswere formed by the oxidation of evaporated zinc vapor in the air. It was found that the particles range from 70 to 100nmin average particle size. The effect of experimental parameters was investigated, the increase of the air flow-rates reduced the average particle size, while increasing the evaporation temperature and the amount of metal charged increased the average particle size. TEM of the particles collected showed that the crystal habits of particles have a tetrapod-like of wurtzite structure consists of four needle crystals. It was found by electron diffraction that all particles were single crystal. Nanometer ZnO particles were synthesized by evaporating of zinc particles of average particle size of 370 μm studied by XRD, TEM and electron diffraction. The particleswere formed by the oxidation of evaporated zinc vapor in the air. It was found that the particles range from 70 to 100nmin average the effect of experimental parameters was investigated, the increase of the air flow-rates reduced the average particle size, while increasing the evaporation temperature and the amount of metal charged increased the average particle size. TEM of the particles collected showed that the crystal habits of particles have a tetrapod-like of wurtzite structure consists of four needle crystals. It was found by electron diffraction that all particles were single crystal.
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