论文部分内容阅读
本文提出一个用气相色谱法测定烷基苯中痕量水份的方法。其特点是:为了定量的需要,在配有水的烷基苯样品中加入2%左右的无水乙醇作标准样,进行外标定量;使用的色谱柱为φ3×2400mm玻璃柱,内装401有机担体。本法测定ppm级水份时,相对误差<±10%,精确度<±5%,一次进样的分析时间为2分钟左右。本方法较卡尔费休法快速简便,测定结果两者相符。此法不需要定量基准,任何烷基苯样品都可以用来配制标样。
This paper presents a method for the determination of trace amounts of water in alkylbenzenes by gas chromatography. Its characteristics are: In order to quantify the need, with water-based alkylbenzene samples by adding about 2% ethanol as a standard sample for external standard quantitation; the use of the column φ3 × 2400mm glass column, containing 401 organic Body. When the method is used to measure ppm level water, the relative error is less than ± 10% and the accuracy is less than ± 5%. The analysis time of one injection is about 2 minutes. This method is faster and easier than the Karl Fischer method, the determination of the results of both. This method does not require a quantitative basis, any alkylbenzene sample can be used to prepare standard.